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Overview of Thermolyne tube furnace

Introduction

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Thermolyne Type 54500 High

Temperature Tube Furnace

Safety

  • Safety training for both use of gas cylinders and the labs must be completed.
  • Safety glasses and long pants must be worn at all times.
  • Fume hoods must be on during all operation when gasses are used.
  • Tubes are made out of ceramic material, alumina in his case, and are affected by thermal shock. Therefore, heating rates no more than 10C are allowed.
  • Furnaces are hot during operation, thus only remove samples after they have returned to room temperature.

Equipment or Bill of Materials

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Thermocouple thermometer

List of necessary components to set up the assembly

Calibration & Tolerances

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Thermocouple - furnace temperature verification


Operation & Procedure

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Example gas to use(N2)
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Primary regulator used on gas supply
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Secondary regulator used on gas supply
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Tube through view with no ends attached
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Gas inlet insulation seal on tube
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Rubber seal close up on gas inlet
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Switch to turn on hood
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Gas inlet attached and sample view from gas outlet
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Gas outlet insulation seal on tube
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Thermocouple and gas outlet with rubber seal
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Gas outlet into hood top
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Furnace interface for programming

Shutdown

References

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