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<u>Reactor configuration</u> | <u>Reactor configuration</u> | ||
# The reactor is placed in an insulated temperature jacket to control the reaction temperature | # The reactor is placed in an insulated temperature jacket to control the reaction temperature. | ||
# The reactor is connected to a reflux condenser and a vacuum pump | # The reactor is connected to a reflux condenser and a vacuum pump. | ||
<u>Polymerization reaction protocol</u> | <u>Polymerization reaction protocol</u> | ||
<u>First step melt polycondensation</u> | <u>First step melt polycondensation</u> |